Publication: Synthesis of PbO Nano-Particles From a New One-Dimensional Lead(II) Coordination Polymer Precursor
| dc.authorscopusid | 35219300600 | |
| dc.authorscopusid | 58038557300 | |
| dc.authorscopusid | 58717985000 | |
| dc.authorscopusid | 36039473500 | |
| dc.contributor.author | Sadeghzadeh, H. | |
| dc.contributor.author | Morsali, A. | |
| dc.contributor.author | Yilmaz, V.T. | |
| dc.contributor.author | Büyuk̈güngör, O. | |
| dc.date.accessioned | 2020-06-21T14:48:40Z | |
| dc.date.available | 2020-06-21T14:48:40Z | |
| dc.date.issued | 2010 | |
| dc.department | Ondokuz Mayıs Üniversitesi | en_US |
| dc.department-temp | [Sadeghzadeh] Homa, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Morsali] Ali, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Yilmaz] Veysel T., Department of Chemistry, Bursa Uludağ Üniversitesi, Bursa, Bursa, Turkey; [Büyuk̈güngör] Orhan, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkey | en_US |
| dc.description.abstract | A new Pb(II) one-dimensional coordination polymer, [Pb(μ-NO<inf>2</inf>)(μ-pyc)(H<inf>2</inf>O)]<inf>n</inf> (1), Hpyc = 2-pyridinecarboxylic acid} was prepared and characterized by elemental analyses, powder XRD diffraction and IR spectroscopy. Compound 1 was structurally characterized by single-crystal X-ray diffraction and one-dimensional coordination polymer with coordination environment of PbNO<inf>6</inf>. The thermal stability of compound 1 showed that compound 1 decomposes at 110-500 °C and the final product is PbO. This polymeric precursor has been used to make PbO nano-particles using two different surfactants. The new nano-structure was characterized by scanning electron microscopy and X-ray powder diffraction. This study demonstrates that the coordination polymers may be suitable precursors for the preparation of nanoscale materials. © 2010 Elsevier B.V. All rights reserved. | en_US |
| dc.identifier.doi | 10.1016/j.matlet.2010.01.017 | |
| dc.identifier.endpage | 813 | en_US |
| dc.identifier.issn | 1873-4979 | |
| dc.identifier.issue | 7 | en_US |
| dc.identifier.scopus | 2-s2.0-76849101386 | |
| dc.identifier.scopusquality | Q2 | |
| dc.identifier.startpage | 810 | en_US |
| dc.identifier.uri | https://doi.org/10.1016/j.matlet.2010.01.017 | |
| dc.identifier.volume | 64 | en_US |
| dc.identifier.wos | WOS:000276190100005 | |
| dc.identifier.wosquality | Q3 | |
| dc.language.iso | en | en_US |
| dc.publisher | Elsevier Science BV | en_US |
| dc.relation.ispartof | Materials Letters | en_US |
| dc.relation.journal | Materials Letters | en_US |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
| dc.rights | info:eu-repo/semantics/closedAccess | en_US |
| dc.subject | Crystal Structure | en_US |
| dc.subject | Nano-Materials | en_US |
| dc.subject | Thermal Properties | en_US |
| dc.title | Synthesis of PbO Nano-Particles From a New One-Dimensional Lead(II) Coordination Polymer Precursor | en_US |
| dc.type | Article | en_US |
| dspace.entity.type | Publication |