Crystal Structure of 3-Acetoxy

Abstract

The structure of 3-acetoxy-2-methyl-N-(4-nitrophenyl)benzamide was determined by X-ray crystallography. The compound crystallized in a monoclinic system and it was characterized in the space group P2<inf>1</inf>/c with cell parameters a = 5.8658(3), b = 17.1661(10), c = 15.1938(7)Å, β = 103.182(4)°s, Z = 4, V = 1489.60(14)Å3. The R1 [I > 2σ(I)] and wR2 (all data) values are 0.046 and 0.093, respectively, for all 2932 independent reflections. Intramolecular C3-H3···O3 and intermolecular N2-H2···O1, C5-H5···O1 interactions were observed in the crystal lattice. © 2018 The Japan Society for Analytical Chemistry.