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Novel Phthalocyanines Containing Substituted Salicyclic Hydrazone-1,3 Moieties: Microwave-Assisted Synthesis, Spectroscopic Characterization, X-Ray Structure and Thermal Characterization

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dc.authorscopusid6602215568
dc.authorscopusid36088434800
dc.authorscopusid8354984000
dc.authorscopusid55907970200
dc.authorscopusid8382150200
dc.authorscopusid6602376941
dc.contributor.authorDeǧirmencioǧlu, I.
dc.contributor.authorAtalay, E.
dc.contributor.authorEr, M.
dc.contributor.authorKöysal, Y.
dc.contributor.authorIşík, S.
dc.contributor.authorSerbest, K.
dc.date.accessioned2020-06-21T14:52:57Z
dc.date.available2020-06-21T14:52:57Z
dc.date.issued2010
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Deǧirmencioǧlu] İsmail, Department of Chemistry, Karadeniz Technical University, Trabzon, Trabzon, Turkey; [Atalay] Esra, Department of Chemistry, Karadeniz Technical University, Trabzon, Trabzon, Turkey; [Er] Mustafa, Department of Chemistry, Karabük Üniversitesi, Karabuk, Turkey; [Köysal] Yavuz, Samsun Vocational School, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Işík] Şamil, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Serbest] Kerim, Department of Chemistry, Recep Tayyip Erdogan University, Rize, Turkeyen_US
dc.description.abstractNovel, metal-free and metallo(Cu, Co, Ni, Zn, Pb and Mn)phthalocyanine compounds were synthesized by exposure to microwave irradiation and the products purified. The newly prepared compounds were characterized using elemental analyses, IR, 1H/13C NMR, 1H-1H COSY measurements, MS, UV-vis spectroscopy and DTA/TG analysis. The electronic spectra exhibited an intense π → π* transition with characteristic Q and B bands of the phthalocyanine core, as expected. All decomposition products obtained from DTA/TG analysis were identified; it was found that the thermal stability of each phthalocyanine compound followed the order: MnPc < Metal-free < ZnPc < PbPc < CuPc < CoPc < NiPc. © 2009 Elsevier Ltd. All rights reserved.en_US
dc.identifier.doi10.1016/j.dyepig.2009.07.001
dc.identifier.endpage78en_US
dc.identifier.issn0143-7208
dc.identifier.issn1873-3743
dc.identifier.issue1en_US
dc.identifier.scopus2-s2.0-69249203454
dc.identifier.scopusqualityQ2
dc.identifier.startpage69en_US
dc.identifier.urihttps://doi.org/10.1016/j.dyepig.2009.07.001
dc.identifier.volume84en_US
dc.identifier.wosWOS:000271375900009
dc.identifier.wosqualityQ1
dc.language.isoenen_US
dc.publisherElsevier Sci Ltden_US
dc.relation.ispartofDyes and Pigmentsen_US
dc.relation.journalDyes and Pigmentsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCharacterizationen_US
dc.subjectHydrazoneen_US
dc.subjectMicrowave Irradiationen_US
dc.subjectPhthalocyanineen_US
dc.subjectSpectroscopyen_US
dc.subjectX-Rayen_US
dc.titleNovel Phthalocyanines Containing Substituted Salicyclic Hydrazone-1,3 Moieties: Microwave-Assisted Synthesis, Spectroscopic Characterization, X-Ray Structure and Thermal Characterizationen_US
dc.typeArticleen_US
dspace.entity.typePublication

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